(S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

Base Information

Chemical Name:(S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate
CAS No.:1313579-16-6
Molecular Formula:C₂₀H₂₀N₂O₅
Molecular Weight:368.389
Hs Code.:

Synonyms:(S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

Suppliers and Price of (S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

Chemical Property:

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Technology Process of (S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

There total 6 articles about (S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313579-14-4
methyl 4-(bromomethyl)-4'-nitrobiphenyl-3-carboxylate

: 6306-52-1
L-valine methylester hydrochloride

: 1313579-16-6
(S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

Guidance literature:: With triethylamine; In toluene; Reflux;

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1313579-16-6
(S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: bromine; iron / 16 h / 0 - 20 °C

2.1: thionyl chloride / 0 - 20 °C

3.1: potassium acetate; bis(pinacol)diborane / palladium diacetate / N,N-dimethyl-formamide / 3 h / 80 °C / Inert atmosphere

3.2: 16 h / 80 °C / Inert atmosphere

4.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 80 °C

5.1: triethylamine / toluene / Reflux

With N-Bromosuccinimide; thionyl chloride; 2,2'-azobis(isobutyronitrile); bromine; potassium acetate; iron; triethylamine; bis(pinacol)diborane; palladium diacetate; In tetrachloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 586-78-7
para-nitrophenyl bromide

: 1313579-16-6
(S)-methyl 3-methyl-2-(6-(4-nitrophenyl)-1-oxoisoindolin-2-yl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate; bis(pinacol)diborane / palladium diacetate / N,N-dimethyl-formamide / 3 h / 80 °C / Inert atmosphere

1.2: 16 h / 80 °C / Inert atmosphere

2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 80 °C

3.1: triethylamine / toluene / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium acetate; triethylamine; bis(pinacol)diborane; palladium diacetate; In tetrachloromethane; N,N-dimethyl-formamide; toluene;