(PhCH(Me)O)₂SiHPh

Base Information

• Chemical Name: (PhCH(Me)O)₂SiHPh
• CAS No.: 199123-29-0
• Molecular Formula: C₂₂H₂₄O₂Si
• Molecular Weight: 348.517
• Mol file: 199123-29-0.mol

Synonyms:(PhCH(Me)O)₂SiHPh

Chemical Property of (PhCH(Me)O)₂SiHPh

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (PhCH(Me)O)₂SiHPh

There total 10 articles about (PhCH(Me)O)₂SiHPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

phenylsilane (694-53-1) + acetophenone (98-86-2) → (PhCH(Me)O)2SiHPh (199123-29-0)

Guidance literature:

With Et₂OFe(catecholate-porous organic polymer); In benzene-d6; at 23 ℃; for 0.0333333h;

DOI:10.1021/cs400043a

Reference yield: 91.0%

phenylsilane (694-53-1) + acetophenone (98-86-2) → (PhCH(Me)O)2SiHPh (199123-29-0) + 1-Phenylethanol (98-85-1,13323-81-4) + (PhCH(Me)O)3SiPh (70061-16-4) + phenyl(1-phenylethoxy)silane

Guidance literature:

With MnN(salen-3,5-tBu₂); In [D₃]acetonitrile; at 80 ℃; for 2h; Time; Sealed tube;

DOI:10.1021/om400805v

Reference yield: 65.0%

1-Phenylethanol (98-85-1,13323-81-4) + phenylsilane (694-53-1) → (PhCH(Me)O)2SiHPh (199123-29-0)

Guidance literature:

With C₂₅H₃₁FeIN₂O; In acetonitrile; at 70 ℃; for 16h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2014.06.005

upstream raw materials:

phenylsilane

acetophenone

Phenyltrichlorosilane

1-Phenylethanol

Downstream raw materials:

1-Phenylethanol