C₂₅H₃₉NO₄Si

Base Information

Chemical Name:C₂₅H₃₉NO₄Si
CAS No.:944059-54-5
Molecular Formula:C₂₅H₃₉NO₄Si
Molecular Weight:445.674
Hs Code.:

C<sub>25</sub>H<sub>39</sub>NO<sub>4</sub>Si

Synonyms:C₂₅H₃₉NO₄Si

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Chemical Property of C₂₅H₃₉NO₄Si

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Technology Process of C₂₅H₃₉NO₄Si

There total 10 articles about C₂₅H₃₉NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 944059-50-1
C₂₁H₃₀O₄

: 7677-24-9
trimethylsilyl cyanide

: 944059-54-5
C₂₅H₃₉NO₄Si

Guidance literature:: With zinc(II) iodide; In dichloromethane; at 20 ℃; for 3.5h;
DOI:10.1021/ol070708j

Reference yield:

: 934749-87-8
3-(2-formyl-3,4,5-trimethoxy-phenyl)-propionic acid methyl ester

: 944059-54-5
C₂₅H₃₉NO₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran; diethyl ether / 2 h / Heating

1.2: 81 percent / tetrahydrofuran; diethyl ether / 2 h / -10 °C

2.1: lithium aluminum hydride / tetrahydrofuran / 0.5 h / -10 °C

3.1: Dess-Martin periodinane; pyridine / CH₂Cl₂ / -10 - 20 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 0 - 20 °C

4.2: 407 mg / tetrahydrofuran; hexane / 15 - 20 °C

5.1: 87 percent / zinc iodide / CH₂Cl₂ / 3.5 h / 20 °C

With pyridine; lithium aluminium tetrahydride; n-butyllithium; Dess-Martin periodane; magnesium; zinc(II) iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 4.2: Wittig reaction;
DOI:10.1021/ol070708j

Reference yield:

: 944059-52-3
C₂₀H₃₂O₅

: 944059-54-5
C₂₅H₃₉NO₄Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: Dess-Martin periodinane; pyridine / CH₂Cl₂ / -10 - 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 0 - 20 °C

2.2: 407 mg / tetrahydrofuran; hexane / 15 - 20 °C

3.1: 87 percent / zinc iodide / CH₂Cl₂ / 3.5 h / 20 °C

With pyridine; n-butyllithium; Dess-Martin periodane; zinc(II) iodide; In tetrahydrofuran; hexane; dichloromethane; 2.2: Wittig reaction;
DOI:10.1021/ol070708j