5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

Base Information

Chemical Name:5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine
CAS No.:142554-09-4
Molecular Formula:C₄₇H₅₈N₄O₁₂Si
Molecular Weight:899.083
Hs Code.:

Synonyms:5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

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Technology Process of 5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

There total 10 articles about 5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilyl-3'-O-levulinylthymidyl)thymidine

: 142554-09-4
5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

Guidance literature:: With sodium metabisulfite; sodium sulfite; In ethanol; water; at 40 ℃; for 48h;
DOI:10.1016/j.bmc.2013.08.058

Reference yield: 70.0%

: 152685-35-3
C₃₈H₄₅F₃N₂O₁₀SSi

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 142554-09-4
5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; for 1h;
DOI:10.1021/jo00079a030

Reference yield:

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 142554-09-4
5'-O-(4,4'-dimethoxytrityl)-3'-O-(5'-O-diisopropylsilylthymidyl)thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole

2: 70 percent / 2,6-di-tert-butyl-4-methylpyridine / 1 h

With 1H-imidazole; 2,6-di-tert-butyl-4-methylpyridine;
DOI:10.1021/jo00079a030