phenyl furan-2-carboxylate

Base Information

• Chemical Name: phenyl furan-2-carboxylate
• CAS No.: 2948-14-3
• Molecular Formula: C11H8 O3
• Molecular Weight: 188.183
• Mol file: 2948-14-3.mol

Synonyms:2-Furoicacid, phenyl ester (6CI,7CI,8CI); NSC 509746; Phenyl 2-furancarboxylate; Phenyl2-furoate

Chemical Property of phenyl furan-2-carboxylate

Chemical Property:

• Vapor Pressure: 0.0021mmHg at 25°C
• Boiling Point: 290.2°Cat760mmHg
• Flash Point: 129.3°C
• Density: 1.209g/cm³

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of phenyl furan-2-carboxylate

There total 29 articles about phenyl furan-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-furancarbonyl chloride (527-69-5) + phenol (108-95-2,27073-41-2) → furan-2-carboxylic acid phenyl ester (2948-14-3)

Guidance literature:

With triethylamine; In dichloromethane; for 0.5h; Reflux;

DOI:10.1002/ejoc.201600714

Reference yield: 96.0%

furfural (98-01-1) + phenol (108-95-2,27073-41-2) → furan-2-carboxylic acid phenyl ester (2948-14-3)

Guidance literature:

With bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-1-ium chloride; palladium diacetate; sodium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; at 100 ℃; for 24h; Sealed tube;

DOI:10.1016/j.tetlet.2011.03.017

Reference yield: 96.0%

2-furancarbonyl chloride (527-69-5) + phenylboronic acid (98-80-6) → furan-2-carboxylic acid phenyl ester (2948-14-3)

Guidance literature:

With oxygen; cesium fluoride; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 5,5-dimethyl-1,3-cyclohexadiene; at 60 ℃; for 12h; under 760.051 Torr;

DOI:10.1002/adsc.201100971

upstream raw materials:

2-furancarbonyl chloride

phenol

2-furanoic acid

2-(((4-methylphenyl)sulfonyl)oxy)benzoic acid

Downstream raw materials:

furan-2-yl(4-hydroxyphenyl)methanone

furan-2-yl(2-hydroxyphenyl)methanone

furan-2-carboxylic acid benzylamide

(furan-2-yl)(phenyl)methanone