Technology Process of trans-1-(1-phenylethylsulfonyl)-2-phenylethene
There total 6 articles about trans-1-(1-phenylethylsulfonyl)-2-phenylethene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 62 percent / K2CO3 / methanol
2.1: 96 percent / NaBO3*4H2O / acetic acid / 12 h / 20 °C
3.1: 74 percent / MsCl / pyridine / 12 h / 20 °C
4.1: nBuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C
4.2: 88 percent / tetrahydrofuran; hexane / 0.17 h / -78 °C
With
sodium perborate; n-butyllithium; potassium carbonate; methanesulfonyl chloride;
In
tetrahydrofuran; pyridine; methanol; hexane; acetic acid;
DOI:10.1002/ejoc.200500956
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 96 percent / NaBO3*4H2O / acetic acid / 12 h / 20 °C
2.1: 74 percent / MsCl / pyridine / 12 h / 20 °C
3.1: nBuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C
3.2: 88 percent / tetrahydrofuran; hexane / 0.17 h / -78 °C
With
sodium perborate; n-butyllithium; methanesulfonyl chloride;
In
tetrahydrofuran; pyridine; hexane; acetic acid;
DOI:10.1002/ejoc.200500956
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C
1.2: 70 percent / tetrahydrofuran / 1.5 h / 20 °C
2.1: nBuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C
2.2: 88 percent / tetrahydrofuran; hexane / 0.17 h / -78 °C
With
n-butyllithium; sodium hydride;
In
tetrahydrofuran; hexane;
1.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1002/ejoc.200500956
