3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

Base Information

Chemical Name:3-(2-methylhexanoyloxy)-4-nitrobenzoic acid
CAS No.:1357303-91-3
Molecular Formula:C₁₄H₁₇NO₆
Molecular Weight:295.292
Hs Code.:

Synonyms:3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

Chemical Property:

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Technology Process of 3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

There total 2 articles about 3-(2-methylhexanoyloxy)-4-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4536-23-6
2-methylhexanoic acid

: 619-14-7
3-hydroxy-4-nitro-benzoic acid

: 1357303-91-3
3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

Guidance literature:: 2-methylhexanoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.5h;

3-hydroxy-4-nitro-benzoic acid; With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃;
DOI:10.1590/S0103-50532011000200016

Reference yield:

: 1357303-90-2
3-(2-bromohexanoyloxy)-4-nitrobenzoic acid

: 1357303-91-3
3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: tris hydrochloride; sodium chloride; calcium chloride / water; acetonitrile / 96 h / 25 °C / pH 8 / Enzymatic reaction

2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 20 °C

With 4-methyl-morpholine; tris hydrochloride; sodium chloride; calcium chloride; isobutyl chloroformate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1590/S0103-50532011000200016

Reference yield:

: 1357303-91-3
3-(2-methylhexanoyloxy)-4-nitrobenzoic acid

: 51703-97-0
(R)-(-)-2-methylhexanoic acid

: 49642-51-5
(S)-(+)-2-methylhexanoic acid

: 619-14-7
3-hydroxy-4-nitro-benzoic acid

Guidance literature:: With tris hydrochloride; sodium chloride; calcium chloride; In water; acetonitrile; at 25 ℃; for 96h; pH=8; Enzymatic reaction;
DOI:10.1590/S0103-50532011000200016