l'α-chloro α-ethoxymethyltributyletain

Base Information

Chemical Name:l'α-chloro α-ethoxymethyltributyletain
CAS No.:79411-60-2
Molecular Formula:C₁₅H₃₃ClOSn
Molecular Weight:383.589
Hs Code.:

Synonyms:l'α-chloro α-ethoxymethyltributyletain

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of l'α-chloro α-ethoxymethyltributyletain

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of l'α-chloro α-ethoxymethyltributyletain

There total 1 articles about l'α-chloro α-ethoxymethyltributyletain which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79411-58-8
diethoxymethyltributylstannane

: 75-36-5
acetyl chloride

: 1461-22-9
tributyltin chloride

: 79411-60-2
l'α-chloro α-ethoxymethyltributyletain

Guidance literature:: In not given; byproducts: ethyl acetate; excess of acetyl chloride added to Bu3SnCH(OEt)2 under N2, stirred at room temp. for 1.5 h, volatiles removed in vacuo; identified by NMR spectra;
DOI:10.1016/S0022-328X(00)99500-7

Reference yield: 72.0%

: 79411-60-2
l'α-chloro α-ethoxymethyltributyletain

: 1730-25-2
allylmagnesium bromide

: 24850-33-7
allyltributylstanane

: 85370-89-4
(α-ethoxybutenyl)tributyltin

Guidance literature:: With water; ammonium chloride; In diethyl ether; to soln. of Bu3SnCHCl(OEt) in anhyd. Et2O added dropwise soln. of CH2CHCH2MgBr in anhyd. Et2O at 0 °C, after 1 h at 0 °C added satd. aq. soln. of NH4Cl; extd. (Et2O), org. layer dried (MgSO4), distd. in vac. or chromd. (SiO2, pentane);
DOI:10.1016/0022-328X(85)87364-2