N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal

Base Information

• Chemical Name: N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal
• CAS No.: 26683-52-3
• Molecular Formula: C₁₁H₁₅ClN₂O₃
• Molecular Weight: 258.705

Synonyms:N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal

Chemical Property of N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal

Chemical Property:

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Technology Process of N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal

There total 1 articles about N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

p-chlorphenylisocyanate (104-12-1) + 2,2-dimethoxyethylamine (22483-09-6) → N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal (26683-52-3)

Guidance literature:

In benzene; at 5 - 20 ℃; for 20h;

DOI:10.3390/molecules26154432

Reference yield: 89.0%

Sesamol (533-31-3) + N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal (26683-52-3) → 1-(4-chlorophenyl)-4-(6-hydroxybenzo[d][1,3]dioxol-5-yl)imidazolidin-2-one

Guidance literature:

With trifluoroacetic acid; In toluene; for 64h; regioselective reaction; Reflux;

DOI:10.3390/molecules26154432

Reference yield: 86.0%

2-hydroxynaphtho-1,4-quinone (83-72-7) + N-(4-Chlorophenyl)carbamoylaminoacetaldehyde dimethyl acetal (26683-52-3) → 2-(1-(4-chlorophenyl)-2-oxoimidazolidin-4-yl)-3-hydroxynaphthalene-1,4-dione

Guidance literature:

With trifluoroacetic acid; In toluene; for 64h; regioselective reaction; Reflux;

DOI:10.3390/molecules26154432

upstream raw materials:

p-chlorphenylisocyanate

2,2-dimethoxyethylamine

Downstream raw materials:

1-(4-Chlorophenyl)imidazolin-2-one

1-(4-Chlorophenyl)-4,5-dimethoxyimidazolidin-2-one

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