Technology Process of (1S-exo)-2-bornyl 2,4-dinitrophenyl sulfone
There total 9 articles about (1S-exo)-2-bornyl 2,4-dinitrophenyl sulfone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium permanganate;
In
acetic acid;
for 22h;
Ambient temperature;
DOI:10.1055/s-1990-26948
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 97 percent / pyridine / 24 h / Ambient temperature
2: 72 percent / propan-2-ol / 13 h / Heating
3: 85 percent / 0.4N NaOH / H2O / Heating
4: 77 percent / benzene / 12 h / Heating
5: 94 percent / KMnO4 / acetic acid / 23 h / Ambient temperature
6: 1) Na metal, (1S-exo)-2-bornanethiol / 1) EtOH, 2a) 13 h, reflux, 2b) 2 h, 5 deg C
7: 29 percent / ethanol / 1a) reflux, 17 h, 1b) 5 deg C, overnight
With
pyridine; sodium hydroxide; potassium permanganate; sodium; (1S,2S,4S)-2-chloro-1-chloromethyl-7,7-dimethylbicyclo[2.2.1]heptane;
In
ethanol; water; acetic acid; isopropyl alcohol; benzene;
DOI:10.1055/s-1990-26948
