2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

Base Information

Chemical Name:2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide
CAS No.:945528-19-8
Molecular Formula:C₁₃H₁₀ClN₃O₃S
Molecular Weight:323.76
Hs Code.:

Synonyms:2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

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Technology Process of 2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

There total 1 articles about 2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 453-72-5
1-fluoro-4-methanesulfonyl-2-nitrobenzene

: 1073-70-7
4-chlorophenylhydrazine hydrochloride

: 945528-19-8
2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

Guidance literature:: With sodium acetate; In ethanol; for 6h; Heating / reflux;

Reference yield: 20.0%

: 945528-19-8
2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

: 945528-21-2
2-(4-chlorophenyl)-5-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole

Guidance literature:: With iron; ammonium chloride; In tetrahydrofuran; water; at 80 ℃; for 3h;

Reference yield:

: 945528-19-8
2-(4-chlorophenyl)-6-(methylsulfonyl)-2H-benzo[d][1,2,3]triazole 1-oxide

: 945528-25-6
2-(4'-chlorophenyl)-5-(ethylsulfonyl)-benzotriazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron; ammonium chloride / tetrahydrofuran; water / 80 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.2: 20 °C

With iron; ammonium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2011.06.047