4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

Base Information

Chemical Name:4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester
CAS No.:175919-79-6
Molecular Formula:C₂₀H₂₂Cl₂N₄O₄
Molecular Weight:453.325
Hs Code.:

Synonyms:4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

Suppliers and Price of 4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

There total 1 articles about 4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 14205-46-0
isopropyl 3-aminocrotonate

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 175919-84-3
2-azidoethyl acetoacetate

: 175919-79-6
4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

Guidance literature:: In isopropyl alcohol; for 6h; Heating;
DOI:10.1002/jhet.5570330127

Reference yield: 26.0%

: 175919-79-6
4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

: 175919-80-9
3-(2-aminoethyl) 5-isopropyl 2,6-dimethyl-1,4-dihydro-4-(2,3-dichlorophenyl)pyridine-3,5-dicarboxylate

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethanol; at 25 ℃; for 1h;
DOI:10.1002/jhet.5570330127

Reference yield:

: 175919-79-6
4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-azido-ethyl) ester 5-isopropyl ester

: 175919-82-1
4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-(2-thioureido-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / H₂ / 5percent Pd/CaCO₃ / ethanol / 1 h / 25 °C

2: 1.) CaCO₃, 2.) NH₃ / 1.) CH₃Cl, H₂O, 25 deg C, 18 h, 2.) MeOH, 0 deg C, 3 h

With ammonia; hydrogen; calcium carbonate; Lindlar's catalyst; In ethanol;
DOI:10.1002/jhet.5570330127