(Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

Base Information

Chemical Name:(Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester
CAS No.:872603-84-4
Molecular Formula:C₂₆H₁₇Cl₃N₂O₄
Molecular Weight:527.791
Hs Code.:

Synonyms:(Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

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Chemical Property of (Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

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Technology Process of (Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

There total 5 articles about (Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-2-hydroxy-propionic acid methyl ester

: 872603-84-4
(Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

: C₂₆H₁₇Cl₃N₂O₄

Guidance literature:: 3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-2-hydroxy-propionic acid methyl ester; With trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; for 0.166667h;

With pyridine; In dichloromethane; at 0 - 20 ℃; for 49h;

Reference yield: 88.0%

: 3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-2-hydroxy-propionic acid methyl ester

: 872603-84-4
(Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

Guidance literature:: With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 - 20 ℃; for 49.1667h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo1017684

Reference yield: 67.0%

: C₂₆H₁₇Cl₃N₂O₄

: 648864-03-3
(E)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid

: 872603-84-4
(Z)-3-[5-benzo[1,3]dioxol-5-yl-1-(2,5-dichloro-phenyl)-1H-pyrazol-3-yl]-2-(3-chloro-phenyl)-acrylic acid methyl ester

Guidance literature:: C₂₆H₁₇Cl₃N₂O₄; With lithium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 3h;

With hydrogenchloride; water; pH=4; stereoselective reaction;
DOI:10.1021/jo1017684