dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

Base Information

Chemical Name:dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate
CAS No.:1373284-92-4
Molecular Formula:C₂₀H₂₂NO₅PS
Molecular Weight:419.438
Hs Code.:

Synonyms:dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

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Chemical Property of dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

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Technology Process of dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

There total 3 articles about dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 70-55-3
toluene-4-sulfonamide

: 66-99-9
β-naphthaldehyde

: 868-85-9
Dimethyl phosphite

: 1373284-92-4
dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

Guidance literature:: With magnesium(II) perchlorate; In neat (no solvent); at 150 ℃; for 0.333333h; chemoselective reaction; Microwave irradiation; Green chemistry;
DOI:10.1016/j.bioorg.2018.09.023

Reference yield: 92.0%

: 36198-87-5
dimethyl trimethylsilyl phosphite

: 17692-84-1
N-(2-naphthylidene)-4-methylbenzenesulfonamide

: 1373284-92-4
dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

Guidance literature:: dimethyl trimethylsilyl phosphite; N-(2-naphthylidene)-4-methylbenzenesulfonamide; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;

With water; In tetrahydrofuran; for 0.5h; Inert atmosphere;
DOI:10.1002/cjoc.201200119

Reference yield: 79.0%

: 17692-84-1
N-(2-naphthylidene)-4-methylbenzenesulfonamide

: 868-85-9
Dimethyl phosphite

: 1373284-92-4
dimethyl (4-methylphenylsulfonamido)(naphthalen-2-yl)methylphosphonate

Guidance literature:: With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0031-1289690