4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Base Information

Chemical Name:4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine
CAS No.:671810-17-6
Molecular Formula:C₂₅H₃₂N₁₂O₅
Molecular Weight:580.606
Hs Code.:

Synonyms:4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Suppliers and Price of 4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

There total 4 articles about 4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100-39-0
benzyl bromide

: 671810-16-5
4,5-O-cyclohexylidine perazidonebramine

: 671810-17-6
4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Guidance literature:: 4,5-O-cyclohexylidine perazidonebramine; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 0.5h;

benzyl bromide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 2h;

Reference yield:

: 933-40-4
cycloxexanone dimethyl ketal

: 671810-17-6
4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Guidance literature:: Multi-step reaction with 2 steps

1: p-tolunesulfonic acid / toluene; acetonitrile / 50 °C / 20 Torr

2: NaH / dimethylformamide

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/anie.200353225

Reference yield:

: 671810-15-4
perazidonebramine

: 671810-17-6
4'-O-benzyl-4,5-O-cyclohexylidine perazidonebramine

Guidance literature:: Multi-step reaction with 2 steps

1: p-tolunesulfonic acid / toluene; acetonitrile / 50 °C / 20 Torr

2: NaH / dimethylformamide

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/anie.200353225