C₂₅H₂₆N₄O₃

Base Information

Chemical Name:C₂₅H₂₆N₄O₃
CAS No.:1558037-03-8
Molecular Formula:C₂₅H₂₆N₄O₃
Molecular Weight:430.506
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₂₅H₂₆N₄O₃

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Chemical Property of C₂₅H₂₆N₄O₃

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Technology Process of C₂₅H₂₆N₄O₃

There total 4 articles about C₂₅H₂₆N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1558038-51-9
C₂₇H₃₂N₄O₄

: 79-10-7
acrylic acid

: 1558037-03-8
C₂₅H₂₆N₄O₃

Guidance literature:: C₂₇H₃₂N₄O₄; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

acrylic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 1558038-47-3
C₁₆H₂₄IN₃O₄

: 1558037-03-8
C₂₅H₂₆N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide / water; 1,4-dioxane / 2 h / Reflux

1.2: 16 h

2.1: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate / N,N-dimethyl-formamide; water / 1.5 h / 140 °C / Microwave irradiation

3.1: triethylamine; pyridine; copper diacetate / dichloromethane / 12 h / -2 °C / Molecular sieve

4.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4.2: 12 h / 20 °C

With pyridine; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); copper diacetate; potassium carbonate; triethylamine; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1558038-48-4
C₁₄H₂₁IN₄O₃

: 1558037-03-8
C₂₅H₂₆N₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate / N,N-dimethyl-formamide; water / 1.5 h / 140 °C / Microwave irradiation

2.1: triethylamine; pyridine; copper diacetate / dichloromethane / 12 h / -2 °C / Molecular sieve

3.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

3.2: 12 h / 20 °C

With pyridine; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); copper diacetate; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;