1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

Base Information

Chemical Name:1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol
CAS No.:102940-76-1
Molecular Formula:C₁₉H₂₆O₂
Molecular Weight:286.414
Hs Code.:

Synonyms:1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

Suppliers and Price of 1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

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Technology Process of 1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

There total 7 articles about 1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1826-67-1
vinyl magnesium bromide

: 102940-75-0
2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxybenzaldehyde

: 102940-76-1
1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja00276a041

Reference yield:

: 6555-40-4
ethyl 2-hydroxy-6-methylbenzoate

: 102940-76-1
1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / NaOH, benzyltriethylammonium chloride / H₂O; CH₂Cl₂ / 5 h / Ambient temperature

2: 80 percent / 1.) lithium diisopropyl amide / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) -78 deg C, 2 h

3: 93 percent / 1.) LiAlH₄; 2.) 10percent aq. NaOH, MgSO₄ / diethyl ether; diethyl ether / 1.) reflux, 1 h; 2.) 0 deg C, then rt., 15 min

4: 80 percent / sodium acetate, PCC / CH₂Cl₂ / 1.5 h / 0 °C

5: 99 percent / tetrahydrofuran / 1 h / 0 °C

With sodium hydroxide; lithium aluminium tetrahydride; N-benzyl-N,N,N-triethylammonium chloride; sodium acetate; magnesium sulfate; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/ja00276a041

Reference yield:

: 6520-83-8
ethyl 2-methoxy-6-methylbenzoate

: 102940-76-1
1-<2-<4-methyl-3-(methylethenyl)-3-pentenyl>-6-methoxyphenyl>-2-propen-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / 1.) lithium diisopropyl amide / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) -78 deg C, 2 h

2: 93 percent / 1.) LiAlH₄; 2.) 10percent aq. NaOH, MgSO₄ / diethyl ether; diethyl ether / 1.) reflux, 1 h; 2.) 0 deg C, then rt., 15 min

3: 80 percent / sodium acetate, PCC / CH₂Cl₂ / 1.5 h / 0 °C

4: 99 percent / tetrahydrofuran / 1 h / 0 °C

With sodium hydroxide; lithium aluminium tetrahydride; sodium acetate; magnesium sulfate; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00276a041