3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine

Base Information

• Chemical Name: 3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine
• CAS No.: 1007098-69-2
• Molecular Formula: C₁₈H₁₄F₂N₄O₂
• Molecular Weight: 356.332

Synonyms:3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine

Chemical Property of 3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine

Chemical Property:

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Technology Process of 3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine

There total 1 articles about 3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]benzonitrile (1007098-68-1) → 3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine (1007098-69-2)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; dimethyl sulfoxide; at 20 ℃; for 70h;

Reference yield:

3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine (1007098-69-2) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → 6-(3,5-difluorophenyl)-2-[3-(5-thioxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)benzyl]-2H-pyridazin-3-one (1007096-86-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 18h;

Reference yield:

3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-N-hydroxybenzamidine (1007098-69-2) + chloroformic acid ethyl ester (541-41-3) → 6-(3,5-difluorophenyl)-2-[3-(5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)benzyl]-2H-pyridazin-3-one (1007096-85-6)

Guidance literature:

With pyridine; In N,N-dimethyl-formamide; at 80 - 100 ℃; for 42h;

upstream raw materials:

3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]benzonitrile

Downstream raw materials:

6-(3,5-difluorophenyl)-2-[3-(5-oxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)benzyl]-2H-pyridazin-3-one

C₂₆H₃₁F₂N₇O₂

6-(3,5-difluorophenyl)-2-[3-(5-thioxo-4,5-dihydro-1,2,4-oxadiazol-3-yl)benzyl]-2H-pyridazin-3-one

6-(3,5-difluorophenyl)-2-[3-(5-trichloromethyl-1,2,4-oxadiazol-3-yl)benzyl]-2H-pyridazin-3-one

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