C₃₀H₂₀FNO₃

Base Information

Chemical Name:C₃₀H₂₀FNO₃
CAS No.:1582776-50-8
Molecular Formula:C₃₀H₂₀FNO₃
Molecular Weight:461.492
Hs Code.:

C<sub>30</sub>H<sub>20</sub>FNO<sub>3</sub>

Synonyms:C₃₀H₂₀FNO₃

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Chemical Property of C₃₀H₂₀FNO₃

Chemical Property:

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Technology Process of C₃₀H₂₀FNO₃

There total 6 articles about C₃₀H₂₀FNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1582776-44-0
C₃₂H₂₄FNO₃

: 1582776-50-8
C₃₀H₂₀FNO₃

Guidance literature:: With potassium hydroxide; In methanol; water; at 50 ℃; for 3h;
DOI:10.1021/ml400521f

Reference yield:

: 2459-25-8
methyl naphthalene-2-carboxylate

: 1582776-50-8
C₃₀H₂₀FNO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluorormethanesulfonic acid; bis-(pyridine)iodonium(I) tetrafluoroborate / dichloromethane / 22 h / 25 °C

2.1: triphenylphosphine; sodium carbonate / tetrahydrofuran; water / 110 °C / Microwave irradiation

3.1: potassium hydroxide / methanol; water / 3 h / 50 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3 h / 25 °C

4.2: 2.5 h / 0 - 25 °C

5.1: (S,S)-1,2-diaminocyclohexane; potassium carbonate; copper(l) iodide / 1,4-dioxane / 17 h / 140 °C / Sealed tube

6.1: potassium hydroxide / methanol; water / 3 h / 50 °C

With copper(l) iodide; trifluorormethanesulfonic acid; bis-(pyridine)iodonium(I) tetrafluoroborate; (S,S)-1,2-diaminocyclohexane; sodium carbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml400521f

Reference yield:

: 1582776-31-5
methyl 5,8-diphenyl-2-naphthoate

: 1582776-50-8
C₃₀H₂₀FNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / methanol; water / 3 h / 50 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3 h / 25 °C

2.2: 2.5 h / 0 - 25 °C

3.1: (S,S)-1,2-diaminocyclohexane; potassium carbonate; copper(l) iodide / 1,4-dioxane / 17 h / 140 °C / Sealed tube

4.1: potassium hydroxide / methanol; water / 3 h / 50 °C

With copper(l) iodide; (S,S)-1,2-diaminocyclohexane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml400521f