benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Base Information

Chemical Name:benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide
CAS No.:1426140-89-7
Molecular Formula:C₃₄H₃₇NO₄P*I
Molecular Weight:681.55
Hs Code.:

Synonyms:benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

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Chemical Property of benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Chemical Property:

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Technology Process of benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

There total 6 articles about benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 119768-48-8
(S)-2-((tert-butoxycarbonyl)amino)-4-iodobutyric acid benzyl ester

: 603-35-0
triphenylphosphine

: 1426140-89-7
benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Guidance literature:: at 80 ℃; for 2h; Inert atmosphere;

Reference yield:

: 1426140-80-8
benzyl 2-(S)-[bis(t-butyloxycarbonyl)amino]-3-(methoxycarbonyl)propanoate

: 1426140-89-7
benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / diethyl ether / 1 h / -78 °C / Inert atmosphere

2: sodium tetrahydroborate; water / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 2 h / 20 °C

4: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 20 °C

5: 2 h / 80 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; cerium(III) chloride heptahydrate; water; iodine; diisobutylaluminium hydride; triphenylphosphine; sodium iodide; In tetrahydrofuran; diethyl ether; acetonitrile;

Reference yield:

: 1426140-81-9
benzyl (S)-2-[bis(t-butyloxycarbonyl)amino]-4-oxobutanoate

: 1426140-89-7
benzyl (S)-2-[(t-butyloxycarbonyl)amino]-4-(triphenylphosphonium)butanoate iodide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate; water / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 2 h / 20 °C

3: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 20 °C

4: 2 h / 80 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; cerium(III) chloride heptahydrate; water; iodine; triphenylphosphine; sodium iodide; In tetrahydrofuran; acetonitrile;