5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

Base Information

Chemical Name:5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin
CAS No.:1612861-16-1
Molecular Formula:C₅₁H₄₄N₄O₂
Molecular Weight:744.936
Hs Code.:

Synonyms:5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

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Chemical Property of 5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

Chemical Property:

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Technology Process of 5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

There total 3 articles about 5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1612861-20-7
5-(4-(4-methoxycarbonylbutyloxy)phenyl)-10,15,20-triphenylporphyrin

: 75-16-1
methylmagnesium bromide

: 1612861-16-1
5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

Guidance literature:: In tetrahydrofuran; diethyl ether; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2014.05.007

Reference yield:

: 1380091-43-9
5-(4-acetoxyphenyl)-10,15,20-triphenylporphyrin

: 1612861-16-1
5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / tetrahydrofuran; methanol / 6 h / Reflux

2.1: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 0.25 h / 60 °C

2.2: 4 h / 60 °C

3.1: tetrahydrofuran; diethyl ether / 6 h / 20 °C / Inert atmosphere

With 18-crown-6 ether; sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide; 2.2: |Williamson Ether Synthesis;
DOI:10.1016/j.tet.2014.05.007

Reference yield:

: 5-(4’-hydroxyphenyl)-10,15,20-triphenylporphyrin

: 1612861-16-1
5-(4-(5-hydroxy-5,5-dimethylpentyloxy)phenyl)-10,15,20-triphenylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 0.25 h / 60 °C

1.2: 4 h / 60 °C

2.1: tetrahydrofuran; diethyl ether / 6 h / 20 °C / Inert atmosphere

With 18-crown-6 ether; potassium carbonate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; 1.2: |Williamson Ether Synthesis;
DOI:10.1016/j.tet.2014.05.007