4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene

Base Information

• Chemical Name: 4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene
• CAS No.: 83831-68-9
• Molecular Formula: C₁₂H₁₆O₄S₂
• Molecular Weight: 288.389
• Mol file: 83831-68-9.mol

Synonyms:4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene

Chemical Property of 4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene

There total 1 articles about 4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

methyl((methylsulfonyl)methyl)sulfane (20163-71-7) + 3,4-dimethoxy-benzaldehyde (120-14-9) → 4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene (83831-68-9)

Guidance literature:

With potassium carbonate; In isopropyl alcohol; for 18h; Heating;

DOI:10.1021/jo00148a038

Reference yield: 88.0%

ethanol (64-17-5) + 4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene (83831-68-9) → ethyl α-ethoxy-α-phenylacetate (79309-63-0)

Guidance literature:

With sulfuric acid; for 18h; Heating;

DOI:10.1021/jo00148a038

Reference yield: 70.0%

4-((E)-2-Methanesulfonyl-2-methylsulfanyl-vinyl)-1,2-dimethoxy-benzene (83831-68-9) → 4-((E)-2-Methanesulfinyl-2-methanesulfonyl-vinyl)-1,2-dimethoxy-benzene (83831-73-6)

Guidance literature:

With dihydrogen peroxide; acetic acid; for 48h; Ambient temperature;

DOI:10.1021/jo00148a038

upstream raw materials:

methyl((methylsulfonyl)methyl)sulfane

3,4-dimethoxy-benzaldehyde

Downstream raw materials:

ethyl α-ethoxy-α-phenylacetate

4-((E)-2-Methanesulfinyl-2-methanesulfonyl-vinyl)-1,2-dimethoxy-benzene

α-(3,4-dimethoxyphenyl)-α-methoxyacetate