Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

Base Information

Chemical Name:Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)
CAS No.:188058-64-2
Molecular Formula:C₃₉H₄₆N₆O₄S₂
Molecular Weight:726.964
Hs Code.:

Synonyms:Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

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Chemical Property of Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

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Technology Process of Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

There total 7 articles about Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2873-74-7
gloutaric dichloride

: 188058-64-2
Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / pyridine / 1) 0 deg C, 1 h; 2) rt, 7 h

2: 80 percent / H₂ / act. Ni / ethanol / 5 h / 80 °C / 75006 Torr

3: 1-ethylpiperidine / tetrahydrofuran / 1) 0 deg C, 1 h; 2) rt, 30 min

4: tetrahydrofuran; methanol / 4 h / Heating

With 1-ethyl-piperidine; pyridine; hydrogen; nickel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/S0223-5234(97)84360-7

Reference yield:

: 22948-02-3
3-aminothiophenol

: 188058-64-2
Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / sodium acetate / ethanol / 36 h / Heating

2: 83 percent / pyridine / 1) 0 deg C, 1 h; 2) rt, 7 h

3: 80 percent / H₂ / act. Ni / ethanol / 5 h / 80 °C / 75006 Torr

4: 1-ethylpiperidine / tetrahydrofuran / 1) 0 deg C, 1 h; 2) rt, 30 min

5: tetrahydrofuran; methanol / 4 h / Heating

With 1-ethyl-piperidine; pyridine; hydrogen; sodium acetate; nickel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/S0223-5234(97)84360-7

Reference yield:

: 93352-49-9
4-amino-2'-nitrodiphenyl sulfide

: 188058-64-2
Pentanedioic acid bis-({3-[2-(3-dimethylamino-propionylamino)-phenylsulfanyl]-phenyl}-amide)

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / pyridine / 1) 0 deg C, 1 h; 2) rt, 7 h

2: 80 percent / H₂ / act. Ni / ethanol / 5 h / 80 °C / 75006 Torr

3: 1-ethylpiperidine / tetrahydrofuran / 1) 0 deg C, 1 h; 2) rt, 30 min

4: tetrahydrofuran; methanol / 4 h / Heating

With 1-ethyl-piperidine; pyridine; hydrogen; nickel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/S0223-5234(97)84360-7