1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

Base Information

Chemical Name:1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride
CAS No.:1622247-27-1
Molecular Formula:C₂₂H₂₄N₂O₂*ClH
Molecular Weight:384.906
Hs Code.:

Synonyms:1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

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Chemical Property of 1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

Chemical Property:

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Technology Process of 1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

There total 7 articles about 1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1622247-25-9
benzyl 4-[2-(5-(benzyloxy)-1H-indol-3-yl)-2-oxoethyl]piperidine-1-carboxylate

: 1622247-27-1
1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; water; for 2h; Reflux;

Reference yield:

: 1953-54-4
indol-5-ol

: 1622247-27-1
1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate; 18-crown-6 ether / acetone / 20 °C

2.1: magnesium; iodine; methyl iodide / diethyl ether / 1 h / 60 °C

2.2: 1.5 h / 0 - 20 °C

3.1: hydrogenchloride / water; ethanol / 2 h / Reflux

With hydrogenchloride; 18-crown-6 ether; iodine; caesium carbonate; magnesium; methyl iodide; In diethyl ether; ethanol; water; acetone;

Reference yield:

: 100-39-0
benzyl bromide

: 1622247-27-1
1-[5-(benzyloxy)-1H-indol-3-yl]-2-(piperidin-4-yl)ethanone hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate; 18-crown-6 ether / acetone / 20 °C

2.1: magnesium; iodine; methyl iodide / diethyl ether / 1 h / 60 °C

2.2: 1.5 h / 0 - 20 °C

3.1: hydrogenchloride / water; ethanol / 2 h / Reflux

With hydrogenchloride; 18-crown-6 ether; iodine; caesium carbonate; magnesium; methyl iodide; In diethyl ether; ethanol; water; acetone;