5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

Base Information

Chemical Name:5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide
CAS No.:173067-74-8
Molecular Formula:C₁₈H₂₀NO₆P
Molecular Weight:377.334
Hs Code.:

Synonyms:5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

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Chemical Property of 5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

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Technology Process of 5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

There total 3 articles about 5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 777-52-6
1-dichlorophosphoryloxy-4-nitro-benzene

: 173067-76-0
2-(1-Methyl-1-phenyl-ethyl)-propane-1,3-diol

: 5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

: 173067-74-8
5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

Guidance literature:: With pyridine; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 6802-75-1
diethyl isopropylidenemalonate

: 173067-74-8
5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 28 percent / diethyl ether; tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) reflux, 1 h

2: 35 percent / LiAlH₄ / diethyl ether / 12 h / Ambient temperature

3: 26 percent / pyridine / tetrahydrofuran / 2 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 78775-63-0
diethyl α-(1-methyl-1-phenylethyl)malonate

: 173067-74-8
5-(1-Methyl-1-phenyl-ethyl)-2-(4-nitro-phenoxy)-[1,3,2]dioxaphosphinane 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / LiAlH₄ / diethyl ether / 12 h / Ambient temperature

2: 26 percent / pyridine / tetrahydrofuran / 2 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;