(tricyclohexylphoshine)AuOAc

Base Information

Chemical Name:(tricyclohexylphoshine)AuOAc
CAS No.:1081979-23-8
Molecular Formula:C₂₀H₃₆AuO₂P
Molecular Weight:536.445
Hs Code.:

Synonyms:(tricyclohexylphoshine)AuOAc

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Chemical Property of (tricyclohexylphoshine)AuOAc

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Technology Process of (tricyclohexylphoshine)AuOAc

There total 1 articles about (tricyclohexylphoshine)AuOAc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 49763-41-9
(tricyclohexylphosphine)gold(I) chloride

: 563-63-3
silver(I) acetate

: 1081979-23-8
(tricyclohexylphoshine)AuOAc

Guidance literature:: In benzene; to soln. Au complex in benzene AgOAc was added, stirred for 2 h; soln. was filtered through Celite and concd. in vacuo, residue was triturated with pentane, ppt. was dried; elem. anal.;
DOI:10.1021/ic3009464

Reference yield: 79.0%

: 4,4,5,5-tetramethyl-2-[7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyren-2-yl]-1,3,2-dioxaborolane

: 1081979-23-8
(tricyclohexylphoshine)AuOAc

: 1189552-36-0
(Au(tricyclohexylphosphine))2(pyrenyl)

Guidance literature:: With cesium carbonate; In tetrahydrofuran; isopropyl alcohol; charging of Schlenk flask with Cs2CO3 in isopropyl alcohol; in separate flask dissolving of Cy3PAuOAc and C16H8(BO2C2Me4)2 in THF; degassing of both solns.; cannulating of THF soln. into Schlenk flask; stirring at 5 0°C for 24 h under Ar; pptn., filtration, washing with isopropanol and THF; slow evapn. of a xylene soln.; crystn., elem. anal.;
DOI:10.1021/om9005214

Reference yield: 39.0%

: 1081979-23-8
(tricyclohexylphoshine)AuOAc

: 147621-18-9
6-indolylboronic acid

: 1391157-79-1
Cy₃PAu(N-indolyl)

Guidance literature:: With Cs₂CO₃; In isopropyl alcohol; to suspn. Cs2CO3 and boronic acid in 2-propanol Au complex was added, stirred at 50°C for 24 h; react. mixt. was cooled and evapd. in vacuo, residue was extd. with toluene, filtered, evapd. in vacuo, residue was triturated with pentane, extd. into toluene and filtered, pentane vapor diffusion; elem. anal.;
DOI:10.1021/ic3009464