bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate)

Base Information

• Chemical Name: bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate)
• CAS No.: 86119-62-2
• Molecular Formula: 2BF₄*C₂₇H₃₂N₄O₃
• Molecular Weight: 634.185

Synonyms:bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate)

Chemical Property of bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate)

There total 4 articles about bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-1H-pyrazole (670-96-2) → bis(N(1)-ethoxymethyl-2-phenyl-N(3)-methylimidazolylium) ketone bis(tetrafluroborate) (86119-62-2)

Guidance literature:

Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran

2: 70 percent / BuLi

3: 82 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 19 h / Ambient temperature

4: CH₂Cl₂ / 0.5 h

With n-butyllithium; sodium acetate; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00354a025

Reference yield:

1-(ethoxymethyl)-2-phenyl-1H-imidazole (86119-53-1) → bis(N(1)-ethoxymethyl-2-phenyl-N(3)-methylimidazolylium) ketone bis(tetrafluroborate) (86119-62-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / BuLi

2: 82 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 19 h / Ambient temperature

3: CH₂Cl₂ / 0.5 h

With n-butyllithium; sodium acetate; pyridinium chlorochromate; In dichloromethane;

DOI:10.1021/ja00354a025

Reference yield:

bis(N-(ethoxymethyl)-2-phenyl-5-imidazolyl)carbinol (86119-54-2) → bis(N(1)-ethoxymethyl-2-phenyl-N(3)-methylimidazolylium) ketone bis(tetrafluroborate) (86119-62-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 19 h / Ambient temperature

2: CH₂Cl₂ / 0.5 h

With sodium acetate; pyridinium chlorochromate; In dichloromethane;

DOI:10.1021/ja00354a025

upstream raw materials:

trimethoxonium tetrafluoroborate

bis(N-(ethoxymethyl)-2-phenyl-5-imidazolyl) ketone

1-(ethoxymethyl)-2-phenyl-1H-imidazole

1-phenyl-1H-pyrazole

Downstream raw materials:

1,1-bis(N-methyl-2-phenyl-4-imidazolyl)-2-(N-methyl-2-imidazolyl)-1-hydroxyethane

bis(N-methyl-2-phenyl-4-imidazolyl) ketone

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 86119-62-2 bis(N⁽¹⁾-ethoxymethyl-2-phenyl-N⁽³⁾-methylimidazolylium) ketone bis(tetrafluroborate)

Send

Send

Metric Ton KG G Pound L ML

Send

Send