2-[4-(ethoxycarbonyl)phenyl]naphthalene

Base Information

Chemical Name:2-[4-(ethoxycarbonyl)phenyl]naphthalene
CAS No.:119999-21-2
Molecular Formula:C₁₉H₁₆O₂
Molecular Weight:276.335
Hs Code.:

Synonyms:2-[4-(ethoxycarbonyl)phenyl]naphthalene

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Chemical Property of 2-[4-(ethoxycarbonyl)phenyl]naphthalene

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-[4-(ethoxycarbonyl)phenyl]naphthalene

There total 13 articles about 2-[4-(ethoxycarbonyl)phenyl]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: (4-(ethoxycarbonyl)phenyl)zinc(II) iodide lithium chloride

: 7433-79-6
2-methylthionaphthalene

: 119999-21-2
2-[4-(ethoxycarbonyl)phenyl]naphthalene

Guidance literature:: (4-(ethoxycarbonyl)phenyl)zinc(II) iodide lithium chloride; With trans-[1,3-bis(2,6-diisopropylphenyl)imidazolin-2-ylidene]PdCl₂(NC₅H₅); In tetrahydrofuran; at 20 ℃; for 0.05h; Inert atmosphere;

2-methylthionaphthalene; In tetrahydrofuran; acetonitrile; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201404380

Reference yield: 84.0%

: 612-55-5
2-iodonaphthalene

: 131379-16-3
4-(ethoxycarbonyl)phenylzinc iodide

: 119999-21-2
2-[4-(ethoxycarbonyl)phenyl]naphthalene

Guidance literature:: With lithium chloride; In tetrahydrofuran; toluene; at 110 ℃; for 48h; Reagent/catalyst; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201308200

Reference yield: 62.0%

: 1192765-24-4
4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N,N-diethylbenzamide

: 61912-15-0
naphthalen-2-yl diisopropylcarbamate

: 119999-21-2
2-[4-(ethoxycarbonyl)phenyl]naphthalene

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 1,3-bis(adamantan-2-yl)imidazolin-2-yliden chloride; sodium ethanolate; In toluene; at 130 ℃; for 20h; Sealed tube; Inert atmosphere;
DOI:10.1016/j.tet.2015.02.088