1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Base Information

Chemical Name:1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone
CAS No.:1300041-64-8
Molecular Formula:C₃₁H₄₃N₃O₄
Molecular Weight:521.7
Hs Code.:

Synonyms:1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Suppliers and Price of 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

There total 6 articles about 1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(8-(2-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-oxoethyl)-7-imino-2,3,4,7,8,9-hexahydro-[1,4]dioxepino[2,3-f]isoindol-3-yl)acetaldehyde trifluoroacetate

: 124-40-3
dimethyl amine

: 1300041-64-8
1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Guidance literature:: 2-(8-(2-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-oxoethyl)-7-imino-2,3,4,7,8,9-hexahydro-[1,4]dioxepino[2,3-f]isoindol-3-yl)acetaldehyde trifluoroacetate; dimethyl amine; With acetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; at 20 ℃; for 3h;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; 1,2-dichloro-ethane; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 300853-66-1
4,5-dihydroxyphthalonitrile

: 1300041-64-8
1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 75 °C

2.1: hydrogen / platinum(IV) oxide / methanol / 24 h / 20 °C / 1810.07 Torr

3.1: N,N-dimethyl-formamide / 18 h / 20 °C

3.2: 0 °C

4.1: acetic acid / 1,2-dichloro-ethane; tetrahydrofuran / 3 h / 20 °C

4.2: 1 h / 20 °C

With hydrogen; acetic acid; triphenylphosphine; diethylazodicarboxylate; platinum(IV) oxide; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; 1.1: Mitsunobu reaction;

Reference yield:

: 1300042-58-3
3-(2,2-diethoxyethyl)-3,4-dihydro-2H-benzo[b][1,4]dioxepine-7,8-dicarbonitrile

: 1300041-64-8
1-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-(3-(2-(dimethylamino)ethyl)-7-imino-3,4-dihydro-[1,4]dioxepino[2,3-f]isoindol-8(2H,7H,9H)-yl)ethanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / platinum(IV) oxide / methanol / 24 h / 20 °C / 1810.07 Torr

2.1: N,N-dimethyl-formamide / 18 h / 20 °C

2.2: 0 °C

3.1: acetic acid / 1,2-dichloro-ethane; tetrahydrofuran / 3 h / 20 °C

3.2: 1 h / 20 °C

With hydrogen; acetic acid; platinum(IV) oxide; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;