C₅₂H₆₆N₄O₁₀Si

Base Information

Chemical Name:C₅₂H₆₆N₄O₁₀Si
CAS No.:1268463-71-3
Molecular Formula:C₅₂H₆₆N₄O₁₀Si
Molecular Weight:935.202
Hs Code.:

C<sub>52</sub>H<sub>66</sub>N<sub>4</sub>O<sub>10</sub>Si

Synonyms:C₅₂H₆₆N₄O₁₀Si

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Chemical Property of C₅₂H₆₆N₄O₁₀Si

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Technology Process of C₅₂H₆₆N₄O₁₀Si

There total 11 articles about C₅₂H₆₆N₄O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268463-59-7
(4aS,11aR,12aS,13S)-8-amino-3,7-bis(benzyloxy)-4a-(tert-butyldimethylsilyloxy)-13-(dimethylamino)-5-hydroxy-10-methoxy-11a,12,12a,13-tetrahydrotetraceno[2,3-d]isoxazole-4,6(4aH,11H)-dione

: 69610-41-9,117625-90-8
Boc-L-Pro-H

: 1268463-71-3
C₅₂H₆₆N₄O₁₀Si

Guidance literature:: (4aS,11aR,12aS,13S)-8-amino-3,7-bis(benzyloxy)-4a-(tert-butyldimethylsilyloxy)-13-(dimethylamino)-5-hydroxy-10-methoxy-11a,12,12a,13-tetrahydrotetraceno[2,3-d]isoxazole-4,6(4aH,11H)-dione; Boc-L-Pro-H; With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In water; 1,2-dichloro-ethane; pH=7; Phosphate buffer;

Reference yield:

: 2785-98-0
2,5-dimethoxybenzoic acid

: 1268463-71-3
C₅₂H₆₆N₄O₁₀Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran / 2.5 h / 0 °C

1.2: 2 h / 25 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 25 °C

3.1: dmap; triethylamine / dichloromethane / 12 h / 25 °C

4.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 20 °C

6.1: acetic anhydride; copper(II) nitrate hydrate / 3 h / 0 - 20 °C

7.1: sodium dithionite / water; tetrahydrofuran / 20 °C

8.1: dmap / N,N-dimethyl-formamide / 5 h / 20 °C

9.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

9.2: 2 h / -100 - -20 °C

10.1: hydrogenchloride / 1,4-dioxane / 20 °C

11.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

11.2: pH 7 / Phosphate buffer

With 2,2,6,6-tetramethyl-piperidine; hydrogenchloride; dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; copper(II) nitrate hydrate; N,N,N,N,-tetramethylethylenediamine; acetic anhydride; boron tribromide; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; triethylamine; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 116324-66-4
2,5-Dimethoxy-6-methylbenzoesaeure

: 1268463-71-3
C₅₂H₆₆N₄O₁₀Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 25 °C

2.1: dmap; triethylamine / dichloromethane / 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 20 °C

5.1: acetic anhydride; copper(II) nitrate hydrate / 3 h / 0 - 20 °C

6.1: sodium dithionite / water; tetrahydrofuran / 20 °C

7.1: dmap / N,N-dimethyl-formamide / 5 h / 20 °C

8.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

8.2: 2 h / -100 - -20 °C

9.1: hydrogenchloride / 1,4-dioxane / 20 °C

10.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.2: pH 7 / Phosphate buffer

With hydrogenchloride; dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; copper(II) nitrate hydrate; N,N,N,N,-tetramethylethylenediamine; acetic anhydride; boron tribromide; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; triethylamine; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;