2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone

Base Information

• Chemical Name: 2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone
• CAS No.: 476443-74-0
• Molecular Formula: C₂₅H₂₈O₄
• Molecular Weight: 392.495

Synonyms:2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone

Chemical Property of 2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone

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Technology Process of 2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone

There total 2 articles about 2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

cyclohexa-1,4-diene (1165952-92-0) + (E)-2-Hydroxy-10-methoxy-6-methoxymethoxymethyl-2-phenyl-dec-6-ene-4,8-diynenitrile (476443-59-1) → 2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone + 2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone (476443-74-0)

Guidance literature:

With triethylamine; In methanol; at 37 ℃;

DOI:10.1016/S0040-4039(02)01529-0

Reference yield: 20.0%

cyclohexa-1,4-diene (1165952-92-0) + Methoxy-acetic acid (E)-1-cyano-9-methoxy-5-methoxymethoxymethyl-1-phenyl-non-5-ene-3,7-diynyl ester (476443-71-7) → 2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone + 2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone (476443-74-0)

Guidance literature:

With triethylamine; In methanol; at 37 ℃; for 0.583333h;

DOI:10.1016/S0040-4039(02)01529-0

Reference yield:

2-cyclohexa-2,4-dienyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone (476443-74-0) → 2-cyclohexyl-2-(5-methoxymethoxymethyl-2-methoxymethyl-phenyl)-1-phenyl-ethanone

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1016/S0040-4039(02)01529-0

upstream raw materials:

cyclohexa-1,4-diene

(E)-2-Hydroxy-10-methoxy-6-methoxymethoxymethyl-2-phenyl-dec-6-ene-4,8-diynenitrile

Methoxy-acetic acid (E)-1-cyano-9-methoxy-5-methoxymethoxymethyl-1-phenyl-non-5-ene-3,7-diynyl ester

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