(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Base Information

Chemical Name:(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide
CAS No.:116386-60-8
Molecular Formula:C₁₈H₃₇NO₄Si
Molecular Weight:359.582
Hs Code.:

Synonyms:(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Chemical Property:

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Technology Process of (1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

There total 9 articles about (1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 116386-60-8
(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / CH₂Cl₂ / 0 °C

2: toluene

With 2,6-dimethylpyridine; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)80074-X

Reference yield:

: 126788-76-9,127062-21-9
(1R,4R,5R)-4-Triisopropylsilanyloxy-6-oxa-bicyclo[3.2.1]octan-7-one

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 116386-60-8
(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Guidance literature:: With trimethylaluminum; In toluene; at 20 ℃;
DOI:10.1021/ja00164a023

Reference yield:

: 4771-80-6
1,2,5,6-tetrahydrobenzoic acid

: 116386-60-8
(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 4 steps

1: m-CPBA / CH₂Cl₂ / 0 °C

2: chlorobenzene / 130 °C

3: 2,6-lutidine / CH₂Cl₂ / 0 °C

4: Al(CH₃)3 / toluene / 20 °C

With 2,6-dimethylpyridine; trimethylaluminum; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chlorobenzene; toluene;
DOI:10.1021/ja00164a023