1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

Base Information

Chemical Name:1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone
CAS No.:1427550-08-0
Molecular Formula:C₂₃H₂₆BrClO₃
Molecular Weight:465.815
Hs Code.:

Synonyms:1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

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Chemical Property of 1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

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Technology Process of 1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

There total 5 articles about 1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1427550-07-9
1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-cyclohexylethanone

: 1427550-08-0
1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

Guidance literature:: With bromine; In 1,4-dioxane; diethyl ether; at 20 ℃; for 0.333333h;

Reference yield:

: 470485-27-9
2-cyclohexyl-1-(2,4-dihydroxyphenyl)ethanone

: 1427550-08-0
1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 17 h / 20 °C / Inert atmosphere

2: tetrabutylammomium bromide; sodium hydroxide / water; 1,2-dichloro-ethane / 49.5 h / Reflux

3: bromine / 1,4-dioxane; diethyl ether / 0.33 h / 20 °C

With tetrabutylammomium bromide; bromine; potassium carbonate; sodium hydroxide; In 1,4-dioxane; diethyl ether; water; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 108-46-3
recorcinol

: 1427550-08-0
1-[4-(benzyloxy)-2-(2-chloroethoxy)phenyl]-2-bromo-2-cyclohexylethanone

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 17 h / 20 °C / Inert atmosphere

3: tetrabutylammomium bromide; sodium hydroxide / water; 1,2-dichloro-ethane / 49.5 h / Reflux

4: bromine / 1,4-dioxane; diethyl ether / 0.33 h / 20 °C

With boron trifluoride diethyl etherate; tetrabutylammomium bromide; bromine; potassium carbonate; sodium hydroxide; In 1,4-dioxane; diethyl ether; water; 1,2-dichloro-ethane; acetonitrile;