29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol

Base Information

• Chemical Name: 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol
• CAS No.: 860030-86-0
• Molecular Formula: C₃₄H₆₀N₂O₁₄
• Molecular Weight: 720.855

Synonyms:29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol

Chemical Property of 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol

Chemical Property:

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Technology Process of 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol

There total 6 articles about 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-(4,4'-dimethoxytrityloxy)-29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosane (860030-85-9) → 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol (860030-86-0)

Guidance literature:

With trichloroacetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 0.0833333h;

DOI:10.1021/ja051179m

Reference yield:

N-(benzyloxycarbonyl)-N'-(bromoacetyl)-1,4-diaminobutane (860030-78-0) → 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol (860030-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / acetonitrile / 0.08 h / 20 °C

1.2: 62 percent / acetonitrile / 1.5 h / 40 °C

2.1: 93 percent / trichloroacetic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C

With sodium hydride; trichloroacetic acid; In 1,2-dichloro-ethane; acetonitrile;

DOI:10.1021/ja051179m

Reference yield:

(4,4'-dimethoxytrityl)decaethylene glycol (860030-74-6) → 29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosan-1-ol (860030-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / acetonitrile / 0.08 h / 20 °C

1.2: 62 percent / acetonitrile / 1.5 h / 40 °C

2.1: 93 percent / trichloroacetic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C

With sodium hydride; trichloroacetic acid; In 1,2-dichloro-ethane; acetonitrile;

DOI:10.1021/ja051179m

upstream raw materials:

1-(4,4'-dimethoxytrityloxy)-29-[N-(1-benzyloxycarbonylamino)butyl]carbamoylmethylenoxy-3,6,9,12,15,18,21,24,27-nonaoxanonacosane

N-(benzyloxycarbonyl)-N'-(bromoacetyl)-1,4-diaminobutane

(4,4'-dimethoxytrityl)decaethylene glycol

Tetraethylene glycol

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