methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate

Base Information

Chemical Name:methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate
CAS No.:1345465-97-5
Molecular Formula:C₁₃H₁₂F₄N₂O₃
Molecular Weight:320.243
Hs Code.:

Synonyms:methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate

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Chemical Property of methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate

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Technology Process of methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate

There total 2 articles about methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 142259-49-2
N-Benzyloxycarbonyl-3,3,3-trifluor-2-<3-(4-fluorphenyl)isoxazol-5-yl>alanin-methylester

: 1345465-97-5
methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 2h;
DOI:10.1039/c1ob06040f

Reference yield:

: 42202-95-9
4-fluoro-N-hydroxybenzimidoyl chloride

: 128970-29-6
2-(Benzyloxycarbonylamino)-2-trifluormethyl-but-3-insaeuremethylester

: 1345465-97-5
methyl 3-[2-(4-fluorophenyl)-2-iminoethylidene]-2-(trifluoromethyl)serinate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; potassium hydrogencarbonate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

With copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; hydrogen; potassium hydrogencarbonate; sodium L-ascorbate; In methanol; water; tert-butyl alcohol;
DOI:10.1039/c1ob06040f