C₃₀H₃₆N₂O₄

Base Information

Chemical Name:C₃₀H₃₆N₂O₄
CAS No.:1256254-54-2
Molecular Formula:C₃₀H₃₆N₂O₄
Molecular Weight:488.627
Hs Code.:

C<sub>30</sub>H<sub>36</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₃₀H₃₆N₂O₄

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Chemical Property of C₃₀H₃₆N₂O₄

Chemical Property:

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Technology Process of C₃₀H₃₆N₂O₄

There total 14 articles about C₃₀H₃₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1155264-46-2
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,4-dihydro-2H-benzo[b][1,4]oxazine

: 1256254-52-0
C₂₂H₂₈ClNO₃

: 1256254-54-2
C₃₀H₃₆N₂O₄

Guidance literature:: With sodium hydrogencarbonate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In ISOPROPYLAMIDE; water; at 130 ℃; for 16h; Inert atmosphere; Sealed tube;

Reference yield:

: 1256254-38-2
C₁₀H₉Cl₂NO₃

: 1256254-54-2
C₃₀H₃₆N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / toluene / 2.5 h / -78 - -35 °C

1.2: -15 °C

2.1: perchloric acid / 6 h / 0 - 5 °C / Sealed tube

2.2: pH 8 - 9

3.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 16 h / 110 °C / Inert atmosphere; Sealed tube

4.1: sodium hydrogencarbonate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / ISOPROPYLAMIDE; water / 16 h / 130 °C / Inert atmosphere; Sealed tube

With perchloric acid; sodium hydrogencarbonate; sodium carbonate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; bis-triphenylphosphine-palladium(II) chloride; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In ISOPROPYLAMIDE; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1154740-67-6
C₈H₇BrClNO

: 1256254-54-2
C₃₀H₃₆N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: potassium acetate / 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere

2: ammonium formate / palladium 10% on activated carbon / methanol / 0.5 h / Reflux

3: sodium hydrogencarbonate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / ISOPROPYLAMIDE; water / 16 h / 130 °C / Inert atmosphere; Sealed tube

With ammonium formate; potassium acetate; sodium hydrogencarbonate; 1,1'-bis-(diphenylphosphino)ferrocene; bis(tri-t-butylphosphine)palladium⁽⁰⁾; palladium 10% on activated carbon; In methanol; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide;