N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

Base Information

Chemical Name:N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol
CAS No.:114040-88-9
Molecular Formula:C₁₆H₂₁NO₂
Molecular Weight:259.348
Hs Code.:

Synonyms:N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

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Chemical Property of N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

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Technology Process of N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

There total 5 articles about N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 114040-87-8
N-benzyl-1,5-dideoxy-1,5-imino-4,6-O-isopropylidene-2,3-di-O-(methylsulfonyl)-D-glucitol

: 114040-88-9
N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

Guidance literature:: With sodium iodide; zinc; In N,N-dimethyl-formamide; at 135 ℃; for 3h;
DOI:10.1016/0008-6215(87)80126-X

Reference yield:

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

: 114040-88-9
N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethylformamide / 2 h

2: 249.3 g / p-toluenesulfonic acid / dimethylformamide; various solvent(s) / 2 h / 30 °C

3: 97 percent / triethylamine / acetone / 6 h / Ambient temperature

4: 70 percent / NaI, Zn / dimethylformamide / 3 h / 135 °C

With potassium carbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; zinc; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(87)80126-X

Reference yield:

: 100-39-0
benzyl bromide

: 114040-88-9
N-benzyl-1,2,3,5-tetradeoxy-1,5-imino-4,6-O-isopropylidene-D-erythro-2-hexenitol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethylformamide / 2 h

2: 249.3 g / p-toluenesulfonic acid / dimethylformamide; various solvent(s) / 2 h / 30 °C

3: 97 percent / triethylamine / acetone / 6 h / Ambient temperature

4: 70 percent / NaI, Zn / dimethylformamide / 3 h / 135 °C

With potassium carbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; zinc; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(87)80126-X