hexanal N-benzoylhydrazone

Base Information

• Chemical Name: hexanal N-benzoylhydrazone
• CAS No.: 372960-01-5
• Molecular Formula: C₁₃H₁₈N₂O
• Molecular Weight: 218.299
• Mol file: 372960-01-5.mol

Synonyms:hexanal N-benzoylhydrazone

Chemical Property of hexanal N-benzoylhydrazone

Chemical Property:

Purity/Quality:

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Technology Process of hexanal N-benzoylhydrazone

There total 1 articles about hexanal N-benzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

benzoic acid hydrazide (613-94-5) + hexanal (66-25-1) → hexanal N-benzoylhydrazone (372960-01-5)

Guidance literature:

In hexane; for 2h; Ambient temperature;

Reference yield: 91.0%

hexanal N-benzoylhydrazone (372960-01-5) → N′-(1-hexyl)benzohydrazide (110452-37-4)

Guidance literature:

With dimethylamine borane; toluene-4-sulfonic acid; In methanol; dichloromethane; at 0 ℃; for 0.7h;

DOI:10.1016/S0040-4020(02)00914-6

Reference yield: 85.0%

danishefsky's diene (54125-02-9) + hexanal N-benzoylhydrazone (372960-01-5) → N-(4-oxo-2-pentyl-3,4-dihydro-2H-pyridin-1-yl)-benzamide

Guidance literature:

danishefsky's diene; hexanal N-benzoylhydrazone; With 5A molecular sieve; Mo₂(OAc)4 activated with O₂; In acetonitrile; at 40 ℃; for 24h;

With methanol; at 20 ℃;

DOI:10.1002/anie.200600801

upstream raw materials:

benzoic acid hydrazide

hexanal

Downstream raw materials:

N′-(1-hexyl)benzohydrazide

Refernces

• 1、 Pei-Lin-Wu,Peng, Shao-Yu,Magrath, Joe. "1-Acyl-2-alkylhydrazines by the Reduction of Acylhydrazones". . p. 435 - 438. Retrieved 2007/10/02.