tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate

Base Information

• Chemical Name: tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate
• CAS No.: 1058165-52-8
• Molecular Formula: C₂₃H₃₇N₅O₁₁
• Molecular Weight: 559.574
• Mol file: 1058165-52-8.mol

Synonyms:tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate

Chemical Property of tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate

There total 1 articles about tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline (1058165-51-7) + [({[(2-methyl-2-propanyl)oxy]carbonyl}amino)oxy]acetic acid (42989-85-5) → tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate (1058165-52-8)

Guidance literature:

[({[(2-methyl-2-propanyl)oxy]carbonyl}amino)oxy]acetic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline; In dichloromethane; Inert atmosphere;

DOI:10.1021/ja804530w

Reference yield: 82.0%

tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate (1058165-52-8) → 2-(aminooxy)-N-(3-(2-(2-(3-(2,4-dinitrophenylamino)propoxy)ethoxy)ethoxy)propyl)acetamide (1180486-07-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ja804530w

upstream raw materials:

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline

[({[(2-methyl-2-propanyl)oxy]carbonyl}amino)oxy]acetic acid

Downstream raw materials:

2-(aminooxy)-N-(3-(2-(2-(3-(2,4-dinitrophenylamino)propoxy)ethoxy)ethoxy)propyl)acetamide