N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline

Base Information

• Chemical Name: N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline
• CAS No.: 1058165-51-7
• Molecular Formula: C₁₆H₂₆N₄O₇
• Molecular Weight: 386.405
• Mol file: 1058165-51-7.mol

Synonyms:N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline

Chemical Property of N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline

There total 1 articles about N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,7,10-trioxa-1,13-diaminotridecane (4246-51-9) + 1-chloro-2,4-dinitro-benzene (97-00-7) → N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline (1058165-51-7)

Guidance literature:

In ethanol; for 2h; Reflux;

Reference yield: 80.0%

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline (1058165-51-7) + C22H20N2O4 (1618102-42-3) → C38H44N6O10

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1039/d0cc04474a

Reference yield: 66.0%

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline (1058165-51-7) + [({[(2-methyl-2-propanyl)oxy]carbonyl}amino)oxy]acetic acid (42989-85-5) → tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate (1058165-52-8)

Guidance literature:

[({[(2-methyl-2-propanyl)oxy]carbonyl}amino)oxy]acetic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

N-(3-(2-(2-(3-aminopropoxy)ethoxy)ethoxy)propyl)-2,4-dinitroaniline; In dichloromethane; Inert atmosphere;

DOI:10.1021/ja804530w

upstream raw materials:

4,7,10-trioxa-1,13-diaminotridecane

1-chloro-2,4-dinitro-benzene

Downstream raw materials:

tert-butyl 16-(2,4-dinitrophenylamino)-2-oxo-7,10,13-trioxa-3-azahexadecyloxycarbamate

C₂₉H₄₆N₆O₁₃

C₂₈H₄₄N₆O₁₃

C₃₂H₄₇N₇O₁₅