methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

Base Information

Chemical Name:methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate
CAS No.:1246523-46-5
Molecular Formula:C₅₂H₅₂N₂O₈
Molecular Weight:832.993
Hs Code.:

methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

Synonyms:methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

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Chemical Property of methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

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Technology Process of methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

There total 34 articles about methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1246523-45-4
methyl 2-(4-(2-azido-3-tert-butoxyphenyl)-6-methoxy-1-(4-methoxyphenethyl)-3,7-bis(4-methoxyphenyl)-1H-indol-2-yl)-2-(4-methoxyphenyl)acetate

: 1246523-46-5
methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

Guidance literature:: In 1,2-dichloro-benzene; for 0.333333h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201001966

Reference yield: 49.0%

: methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-hydroxy-2-(4-methoxyphenyl)acetate

: 1246523-46-5
methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; In isopropyl alcohol; at 20 ℃;
DOI:10.1002/chem.202001950

Reference yield:

: 14425-64-0
4-methoxyphenethyl bromide

: 1246523-46-5
methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 2 h

2.1: silver trifluoromethanesulfonate / tetrahydrofuran / 2 h / -78 °C

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / Reflux

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / 1,4-dioxane; water / 0.33 h / Reflux

5.1: 1,2-dichloro-benzene / 0.33 h / Inert atmosphere; Reflux

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; silver trifluoromethanesulfonate; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; 4.1: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201000544