methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Base Information

Chemical Name:methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate
CAS No.:1246523-47-6
Molecular Formula:C₅₀H₄₅Cl₃N₂O₁₁S
Molecular Weight:988.339
Hs Code.:

methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Synonyms:methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

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Chemical Property of methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

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Technology Process of methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

There total 25 articles about methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 764-09-0
chlorosulfuric acid 2,2,2-trichloroethyl ester

: 1246523-57-8
methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

: 1246523-47-6
methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/anie.201001966

Reference yield:

: 1246523-44-3
2-azido-1-tert-butoxy-3-iodobenzene

: 1246523-47-6
methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / 1,4-dioxane; water / 0.33 h / Reflux

2: 1,2-dichloro-benzene / 0.33 h / Inert atmosphere; Reflux

3: boron trichloride / dichloromethane; pentamethylbenzene, / 0.42 h / -78 °C

4: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane / 2 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; boron trichloride; sodium hydroxide; In 1,4-dioxane; dichloromethane; pentamethylbenzene,; water; 1,2-dichloro-benzene; 1: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201000544

Reference yield:

: 1246523-46-5
methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

: 1246523-47-6
methyl 2-(5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-7-(2,2,2-trichloroethoxysulfonyloxy)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trichloride / dichloromethane; pentamethylbenzene, / 0.42 h / -78 °C

2: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane / 2 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; boron trichloride; In dichloromethane; pentamethylbenzene,;
DOI:10.1002/asia.201000544