methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Base Information

Chemical Name:methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate
CAS No.:1246523-57-8
Molecular Formula:C₄₈H₄₄N₂O₈
Molecular Weight:776.886
Hs Code.:

Synonyms:methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

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Chemical Property of methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

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Technology Process of methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

There total 30 articles about methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1246523-46-5
methyl 2-{7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl}-2-(4-methoxyphenyl)acetate

: 1246523-57-8
methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Guidance literature:: With pentamethylbenzene,; boron trichloride; In dichloromethane; at -78 ℃;
DOI:10.1002/anie.201001966

Reference yield:

: C₅₅H₅₀N₂O₈

: 1246523-57-8
methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethyl acetate; at 50 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ja512059d

Reference yield:

: 1246523-45-4
methyl 2-(4-(2-azido-3-tert-butoxyphenyl)-6-methoxy-1-(4-methoxyphenethyl)-3,7-bis(4-methoxyphenyl)-1H-indol-2-yl)-2-(4-methoxyphenyl)acetate

: 1246523-57-8
methyl 2-(7-hydroxy-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)-2-(4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dichloro-benzene / 0.33 h / Inert atmosphere; Reflux

2: boron trichloride / dichloromethane; pentamethylbenzene, / 0.42 h / -78 °C

With boron trichloride; In dichloromethane; pentamethylbenzene,; 1,2-dichloro-benzene;
DOI:10.1002/asia.201000544