7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

Base Information

Chemical Name:7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone
CAS No.:911286-05-0
Molecular Formula:C₂₈H₂₄O₈
Molecular Weight:488.494
Hs Code.:

Synonyms:7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

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Chemical Property of 7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

Chemical Property:

Purity/Quality:

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Technology Process of 7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

There total 12 articles about 7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 911285-98-8
5,7-dihydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

: 98-88-4
benzoyl chloride

: 911286-05-0
7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

Guidance literature:: With potassium carbonate; In acetone; at 45 ℃; for 0.416667h;
DOI:10.1016/j.tet.2006.06.066

Reference yield:

: 911286-03-8
5,7-bis(benzyloxy)-6-iodo-3',4'-methylenedioxyisoflavone

: 911286-05-0
7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Et₃N; PdCl₂; PPh₃ / CuI / dimethylformamide / 0.13 h / 80 °C / microwave irradiation

2: 87 percent / H₂ / Pd/C / methanol; dioxane / 1 h / 20 °C

3: 91 percent / K₂CO₃ / acetone / 0.42 h / 45 °C

With hydrogen; potassium carbonate; triethylamine; triphenylphosphine; palladium dichloride; palladium on activated charcoal; copper(l) iodide; In 1,4-dioxane; methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2006.06.066

Reference yield:

: 2',4'-bis(benzyloxy)-6'-hydroxy-3'-iodo-3,4-methylenedioxychalcone

: 911286-05-0
7-benzoyloxy-5-hydroxy-6-(3-hydroxy-3-methylbutyl)-3',4'-methylenedioxyisoflavone

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / pyridine / 0.1 h / 125 °C / microwave irradiation

2: [hydroxy(tosyloxy)iodo]benzene / CHCl₃ / 0.2 h / 60 °C / microwave irradiation

3: 0.78 g / aq. NaOH / methanol; CHCl₃ / 0.08 h / 50 °C / microwave irradiation

4: 68 percent / Et₃N; PdCl₂; PPh₃ / CuI / dimethylformamide / 0.13 h / 80 °C / microwave irradiation

5: 87 percent / H₂ / Pd/C / methanol; dioxane / 1 h / 20 °C

6: 91 percent / K₂CO₃ / acetone / 0.42 h / 45 °C

With pyridine; sodium hydroxide; [hydroxy(tosyloxy)iodo]benzene; hydrogen; potassium carbonate; triethylamine; triphenylphosphine; palladium dichloride; palladium on activated charcoal; copper(l) iodide; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2006.06.066