N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane

Base Information

Chemical Name:N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane
CAS No.:849453-91-4
Molecular Formula:C₁₅H₃₂ClN₂PSi₃
Molecular Weight:391.116
Hs Code.:

Synonyms:N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane

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Technology Process of N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane

There total 1 articles about N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 22846-03-3
N-lithio-N,N',N'-[tris(trimethylsilyl)]hydrazide

: 644-97-3
Dichlorophenylphosphine

: 849453-91-4
N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane

Guidance literature:: In diethyl ether; at -40 - 20 ℃; Inert atmosphere;
DOI:10.1021/ic200005q

Reference yield: 60.0%

: 849453-91-4
N,N',N'-tris(trimethylsilyl)hydrazino(chloro)phenylphosphane

: 13450-90-3
Gallium trichloride

: 1271313-66-6
Cl(CH₃)2Si((CH₃)3Si)NN(Si(CH₃)3)P(C₆H₅)(CH₃)GaCl₃

Guidance literature:: In dichloromethane; under Ar, Schlenk technique; soln. of GaCl3 in CH2Cl2 added dropwise to soln. of hydrazinophosphane in CH2Cl2 at -70°C under stirring, soln. warmed to room temp., stirred for 12 h; concd. under vac., stored at -25°C for 12 h, supernatant removed by syringe, residue washed with hexane, dried under vac.; elem. anal.;
DOI:10.1021/ic200005q