ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate

Base Information

Chemical Name:ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate
CAS No.:1315342-50-7
Molecular Formula:C₂₈H₃₆BF₂NO₄
Molecular Weight:499.406
Hs Code.:

Synonyms:ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate

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Chemical Property of ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate

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Technology Process of ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate

There total 2 articles about ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1315342-48-3
ethyl 2-N-(diphenylmethyleneamino)-2-(difluoromethyl)-hex-5-enoate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1315342-50-7
ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; bis-diphenylphosphinomethane; In dichloromethane; at 25 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jm200443b

Reference yield:

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 1315342-50-7
ethyl 2-N-(diphenylmethyleneamino)-2-difluoromethyl-6-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.92 h / -78 - 20 °C / Inert atmosphere

3.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; bis-diphenylphosphinomethane / dichloromethane / 18 h / 25 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium tert-butylate; bis-diphenylphosphinomethane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm200443b