4-cyano-6,6,6-trifluorohexyl benzoate

Base Information

Chemical Name:4-cyano-6,6,6-trifluorohexyl benzoate
CAS No.:1512840-63-9
Molecular Formula:C₁₄H₁₄F₃NO₂
Molecular Weight:285.266
Hs Code.:

Synonyms:4-cyano-6,6,6-trifluorohexyl benzoate

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Chemical Property of 4-cyano-6,6,6-trifluorohexyl benzoate

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Technology Process of 4-cyano-6,6,6-trifluorohexyl benzoate

There total 3 articles about 4-cyano-6,6,6-trifluorohexyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 887144-94-7
Togni's reagent II

: 7677-24-9
trimethylsilyl cyanide

: 29264-40-2
5-pentenylbenzoate

: 1512840-63-9
4-cyano-6,6,6-trifluorohexyl benzoate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dimethyl sulfoxide; at 60 ℃; for 0.5h; Mechanism; Inert atmosphere;
DOI:10.1021/ol403263c

Reference yield: 77.0%

: 7677-24-9
trimethylsilyl cyanide

: 29264-40-2
5-pentenylbenzoate

: 2926-29-6
Langlois reagent

: 1512840-63-9
4-cyano-6,6,6-trifluorohexyl benzoate

Guidance literature:: With sodium persulfate; copper(II) nitrate trihydrate; In water; dimethyl sulfoxide; at 90 ℃; for 1h; Sealed tube; Microwave irradiation;
DOI:10.1021/acs.joc.8b02073

Reference yield:

: 821-09-0
n-Pent-4-enyl alcohol

: 98-88-4
benzoyl chloride

: 1512840-63-9
4-cyano-6,6,6-trifluorohexyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 0 - 20 °C

2: copper(II) bis(trifluoromethanesulfonate) / dimethyl sulfoxide / 0.5 h / 60 °C / Inert atmosphere

With pyridine; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol403263c