1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane

Base Information

• Chemical Name: 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane
• CAS No.: 1266399-82-9
• Molecular Formula: C₃₀H₃₆N₆O₄S₂
• Molecular Weight: 608.786

Synonyms:1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane

Chemical Property of 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane

Chemical Property:

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Technology Process of 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane

There total 4 articles about 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

ethyl bromoacetate (105-36-2) + C22H24N6S2 (64546-22-1) → 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane (1266399-82-9)

Guidance literature:

With potassium carbonate; In acetone; for 8h; Reflux;

DOI:10.1007/s00044-010-9517-9

Reference yield:

1-isothiocyanato-4-methylbenzene (622-59-3) → 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane (1266399-82-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Reflux

2: Heating; Alkaline conditions

3: acetone / Reflux

In acetone;

DOI:10.1002/ardp.201000177

Reference yield:

adipic acid dihydrazide (1071-93-8,98152-55-7) → 1,4-bis-[5-(carbethoxymethyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane (1266399-82-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Reflux

2: Heating; Alkaline conditions

3: acetone / Reflux

In acetone;

DOI:10.1002/ardp.201000177

upstream raw materials:

4,4'-di-p-tolyl-1,1'-hexanedioyl-bis-thiosemicarbazide

ethyl bromoacetate

C₂₂H₂₄N₆S₂

1-isothiocyanato-4-methylbenzene

Downstream raw materials:

1,4-bis[5-(1-oxo-1-(3,5-dimethylpyrazol-1-yl)methyl)thio-4-(p-tolyl)-1,2,4-triazol-3-yl]butane

1,4-bis[5-(hydrazinocarbonylmethyl)thio-4-p-tolyl-1,2,4-triazol-3-yl]butane

1,4-bis[5-(5-mercapto-1,3,4-oxadiazol-2-yl-methyl)-thio-4-(p-tolyl)-1,2,4-triazol-3-yl]-butane

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