C₁₅H₂₀INO₅

Base Information

Chemical Name:C₁₅H₂₀INO₅
CAS No.:1385774-56-0
Molecular Formula:C₁₅H₂₀INO₅
Molecular Weight:421.232
Hs Code.:

C<sub>15</sub>H<sub>20</sub>INO<sub>5</sub>

Synonyms:C₁₅H₂₀INO₅

Suppliers and Price of C₁₅H₂₀INO₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀INO₅

Chemical Property:

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Technology Process of C₁₅H₂₀INO₅

There total 3 articles about C₁₅H₂₀INO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 128033-28-3
methyl 2-hydroxy-3-iodobenzoate

: 39684-80-5
2-(tert-butoxycarbonylamino)ethyl bromide

: 1385774-56-0
C₁₅H₂₀INO₅

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c2ob25618e

Reference yield:

: 533-58-4
2-Iodophenol

: 1385774-56-0
C₁₅H₂₀INO₅

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; magnesium chloride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux

2: sodium cyanide; manganese(IV) oxide; acetic acid / 12 h / 20 °C / Inert atmosphere

3: caesium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

With sodium cyanide; manganese(IV) oxide; caesium carbonate; acetic acid; triethylamine; magnesium chloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25618e

Reference yield:

: 23602-64-4
2-hydroxy-3-iodo-benzaldehyde

: 1385774-56-0
C₁₅H₂₀INO₅

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanide; manganese(IV) oxide; acetic acid / 12 h / 20 °C / Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

With sodium cyanide; manganese(IV) oxide; caesium carbonate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1039/c2ob25618e