(E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

Base Information

Chemical Name:(E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide
CAS No.:1446891-97-9
Molecular Formula:C₁₁H₁₅N₃O₃S
Molecular Weight:269.324
Hs Code.:

Synonyms:(E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

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Technology Process of (E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

There total 1 articles about (E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.4%

: 6610-29-3
4-methylthiosemicarbazide

: 134-96-3
syringic aldehyde

: 1446891-97-9
(E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

Guidance literature:: In neat (no solvent); at 140 - 160 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2013.04.043

Reference yield: 92.6%

: 1446891-97-9
(E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 1446892-01-8
(E)-ethyl-2-((E)-(4-hydroxy-3,5-dimethoxy benzylidene)hydrazono)-3,4-dimethyl-2,3-dihydro-thiazole-5-carboxylate

Guidance literature:: In ethanol; for 72h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1016/j.jorganchem.2013.04.043

Reference yield:

: 1446891-97-9
(E)-2-(4-hydroxy-3,5-dimethoxybenzylidene)-N-methylhydrazinecarbothioamide

: 1446892-05-2
(E)-ethyl 2-((E)-(4-(3,4-dicyanophenoxy)-3,5-dimethoxybenzylidene)hydrazono)-3,4-dimethyl-2,3-dihydrothiazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 72 h / Inert atmosphere; Schlenk technique; Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 120 h / 60 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.jorganchem.2013.04.043